5,5-二甲基-1,3-环己二酮合成路线 (共 504 条)
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Davis,B.R.; Woodgate,P.D.
Journal of the Chemical Society, 1965 , p. 5943 - 5948
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Dey; Linstead
Journal of the Chemical Society, 1935 , p. 1063
参考文献
Auterinen
Suomen Kemistilehti B, 1954 , vol. 27, p. 29,32
反应条件
in benzene T=20°C; 2.5 h;
参考文献
Levchenko, E. S.; Budnik, L. V.; Kalinin, V. N.; Kisilenko, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 12 p. 2249 - 2251
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 12 p. 2549 - 2552
反应条件
1: DCC, DMAP 2: TFA / ethanol / 60 h / Heating View Scheme
参考文献
Walton, Tashfeen; Bradley, Mark; Dhaliwal, Kev; Avlonitis, Nikolaos; Haslett, Chris; McDonald, Neil; Debunne, Manuelle
Patent: US2014/134110 A1, 2014 ;
反应条件
in benzene T=20°C; 2.5 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, # 12 p. 2249 - 2251
Zhurnal Organicheskoi Khimii, , vol. 18, # 12 p. 2549 - 2552
反应条件
in benzene 6 h; Heating;
参考文献
Schank, Kurt; Blattner, Rudolf; Schmidt, Volker; Hasenfratz, Hermann
Chemische Berichte, 1981 , vol. 114, # 5 p. 1938 - 1950
反应条件
bromine; acetic acid T=20°C; 2 h;
参考文献
UCB PHARMA S.A.
Patent: WO2009/71895 A1, 2009 ;
Location in patent: Page/Page column 95-96 ;
WO 2009/071895 A1
反应条件
bromine complrex of poly(styrene-co-4-vinylpyridine); dibenzoyl peroxide in tetrachloromethane 4 h; Heating;
参考文献
Sket, Boris; Zupan, Marko
Synthetic Communications, 1989 , vol. 19, # 13-14 p. 2481 - 2488
参考文献
Crossley
Journal of the Chemical Society, 1899 , vol. 75, p. 775
Full Text Show Details
Vorlaender; Kohlmann
Justus Liebigs Annalen der Chemie, 1902 , vol. 322, p. 256