5,5-二甲基-1,3-环己二酮合成路线 (共 504 条)
反应条件
butyric acid sodium salt
参考文献
Inagaki et al.
Yakugaku Zasshi, 1956 , vol. 76, p. 1258
Chem.Abstr., 1957 , p. 4308
反应条件
1: 70 percent / potassium carbonate / CHCl3 / 48 h / 20 °C 2: 86 percent / acetic acid / 12 h / Heating View Scheme
参考文献
Gonzalez-Chavez, Rodolfo; Martinez, Roberto; Torre-Bouscoulet, Maria Eugenia; Gallo, Marco; Gonzalez-Chavez, Marco Martin
Chemical and Pharmaceutical Bulletin, 2014 , vol. 62, # 1 p. 16 - 24
反应条件
Sc(DS)3 in water T=40°C; Friedlaender annulation;
参考文献
Zhang, Liang; Wu, Jie
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 7 p. 1047 - 1051
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in water; acetonitrile 24 h; Ambient temperature;
参考文献
Bassetti, Mauro; Cerichelli, Giorgio; Floris, Barbara
Gazzetta Chimica Italiana, 1986 , vol. 116, # 10 p. 583 - 586
反应条件
12-tungestocobaltic acid supported on nano silica T=80°C; 0.25 h; neat (no solvent);
参考文献
Rafiee, Ezzat; Khodayari, Maryam; Kahrizi, Masoud; Tayebee, Reza
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 358, p. 121 - 128
参考文献
Bilbao, Estibaliz R.; Alvarado, Mario; Masaguer, Christian F.; Ravina, Enrique
Tetrahedron Letters, 2002 , vol. 43, # 19 p. 3551 - 3554
反应条件
in various solvent(s) 24 h; Irradiation;
参考文献
Saito, Kimitoshi; Yuki, Hidetaka; Ohyama, Toshiyuki; Nakane, Ryohei; Nagumo, Katsuyuki; Sato, Tadashi
Canadian Journal of Chemistry, 1981 , vol. 59, p. 1717 - 1721
反应条件
in acetic acid Cyclization; 30 h; Heating;
参考文献
Suarez, Margarita; Ochoa, Estael; Verdecia, Yamila; Pita,Beatriz; Moran, Lourdes; et al.
Tetrahedron, 1999 , vol. 55, # 3 p. 875 - 884
反应条件
oxalyl dichloride in N,N-dimethyl-formamide T=0 - 20°C; 1 h;
参考文献
Mehta, Goverdhan; Bera, Mrinal K.
Tetrahedron, 2013 , vol. 69, # 7 p. 1815 - 1821
反应条件
thionyl chloride in benzene T=25°C; 2 weeks;
参考文献
Journal of Organic Chemistry, , vol. 46, # 24 p. 4911 - 4914