5,5-二甲基-1,3-环己二酮合成路线 (共 504 条)
反应条件
1: DCC, DMAP 2: 64 percent / TFA / ethanol / 60 h / Heating View Scheme
参考文献
Chhabra, Siri Ram; Hothi, Bhupinder; Evans, David J.; White, Peter D.; Bycroft, Barrie W.; Chan, Weng C.
Tetrahedron Letters, 1998 , vol. 39, # 12 p. 1603 - 1606
反应条件
1: triethylamine, tosyl azide / CH2Cl2 / 3 h / 0 °C 2: 94 percent / acetonitrile / 2 h / Irradiation View Scheme
参考文献
Cossy, Janine; Belotti, Damien; Bouzide, Abderahim; Thellend, Annie
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 723 - 729
反应条件
in benzene 1.5 h; Heating;
参考文献
Moehrle, Hans; Arz, Petra
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 8 p. 1035 - 1046
反应条件
1: 41 percent / anhyd. K2CO3 / CHCl3 / 18 h / 28 °C 2: 80 percent / conc. H2SO4 / ethanol / 3 h / Heating 3: chlorobenzene / 3 h / Heating View Scheme
参考文献
Nagarajan; Shenoy; Talwalker
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 4 p. 326 - 332
反应条件
potassium carbonate in chloroform T=20°C; 48 h;
参考文献
Martinez, Roberto; Arzate, Martha Menes; Ramirez-Apan, Ma. Teresa
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 5 p. 1849 - 1856
反应条件
potassium carbonate in chloroform T=25°C; 12 h;
参考文献
Maini, Prem Nath; Sammes, Michael P.; Katritzky, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 161 - 168
反应条件
tert.-butylhydroperoxide in water T=80°C; 4 h; Inert atmosphere; stereoselective reaction;
参考文献
Saberi, Dariush; Heydari, Akbar
Tetrahedron Letters, 2013 , vol. 54, # 32 p. 4178 - 4180
参考文献
Geigy A.G.
Patent: DE826133 , 1949 ;
DRP/DRBP Org.Chem.
反应条件
tetrakis(triphenylphosphine) palladium(0) in methanol
参考文献
Lapitskaya, M. A.; Pivnitskii, K. K.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 9.2 p. 1665 - 1668
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 9 p. 1926 - 1929
反应条件
potassium hydroxide; copper
参考文献
Lukes; Hofman
Collection of Czechoslovak Chemical Communications, 1958 , vol. 23, p. 1110,1118