5,5-二甲基-1,3-环己二酮合成路线 （共 504 条）
参考文献
Desai
Journal of the Chemical Society, 1932 , p. 1079,1086
参考文献
Ahluwalia, V. K.; Rao, J. Shailaja
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 81 - 82
反应条件
1: With potassium hydroxide in methanol T=0 - 20°C; 16 h; 2: With methanol; sodium hydroxide; water T=20°C; 4 h; 3: With hydrogenchloride; water in methanol
参考文献
NOVARTIS AG
Patent: WO2008/101905 A1, 2008 ;
Location in patent: Page/Page column 20-21 ;
WO 2008/101905 A1
反应条件
silica boron-sulfuric acid nanoparticles in neat (no solvent)
T=50°C; 3 h; Green chemistry;
参考文献
Khalafi-Nezhad, Ali; Panahi, Farhad; Mohammadi, Somayeh; Foroughi, Habib Ollah
Journal of the Iranian Chemical Society, 2013 , vol. 10, # 2 p. 189 - 200
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=15°C; 15 h;
参考文献
Prager, Rolf H.; Were, Stephen T.
Australian Journal of Chemistry, 1991 , vol. 44, # 11 p. 1635 - 1641
反应条件
potassium cyanide; triethylamine in acetonitrile
参考文献
Montes, Imber Flores; Burger, Ulrich
Tetrahedron Letters, 1996 , vol. 37, # 7 p. 1007 - 1010
参考文献
Dagher, C.; Hanna, R.; Terentiev, P. B.; Boundel, Y. G.; Kost, A. N.; Maksimov, B. I.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 645 - 647
反应条件
potassium carbonate in chloroform
T=25°C; 12 h; cyclic diketones with var. α-bromo ketones; Product distribution;
参考文献
Maini, Prem Nath; Sammes, Michael P.; Katritzky, Alan R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 161 - 168
反应条件
hydroxylamine hydrochloride; silica gel
T=50°C; 4 h; Green chemistry; Temperature;
参考文献
Ghosh, Pranab; Subba, Raju
Journal of the Indian Chemical Society, 2013 , vol. 90, # 4 p. 529 - 532
反应条件
T=20°C; Solid phase reaction; condensation; 0.5 h;
参考文献
Kaupp, Gerd; Schmeyers, Jens; Boy, Juergen
Advanced Synthesis and Catalysis, 2000 , vol. 342, # 3 p. 269 - 280
