5,5-二甲基-1,3-环己二酮合成路线 （共 504 条）
反应条件
ammonium acetate in water
T=20°C; Green chemistry;
参考文献
Gawande, Manoj B.; Bonifacio, Vasco D. B.; Varma, Rajender S.; Nogueira, Isabel D.; Bundaleski, Nenad; Ghumman, C. Amjad A.; Teodoro, Orlando M. N. D.; Branco, Paula S.
Green Chemistry, 2013 , vol. 15, # 5 p. 1226 - 1231
反应条件
hydrogenchloride in N,N-dimethyl-formamide
Heating;
参考文献
Chebanov; Saraev; Kobzar'; Desenko; Orlov; Gura
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 4 p. 475 - 480
反应条件
hydrogenchloride in N,N-dimethyl-formamide
3 h; Heating;
参考文献
Chebanov; Saraev; Kobzar'; Desenko; Orlov; Gura
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 4 p. 475 - 480
反应条件
tert-butylhypochlorite; triethylamine
1.) benzene, 15 min, 2.) benzene, RT, 8 h; Yield given. Multistep reaction;
参考文献
Wilson, R. Marchall; Hengge, Alvan
Journal of Organic Chemistry, 1987 , vol. 52, # 13 p. 2699 - 2707
反应条件
XeF2; polystyrene-4-vinylpyridine*BF3; hydrogen fluoride in dichloromethane
20 h; Ambient temperature;
参考文献
Zajc, Barbara; Zupan, Marko
Journal of the Chemical Society, Chemical Communications, 1980 , # 16 p. 759 - 760
反应条件
fluorine in formic acid
T=10 - 15°C; 2 h;
参考文献
Chambers, Richard D.; Greenhall, Martin P.; Hutchinson, John
Journal of the Chemical Society, Chemical Communications, 1995 , # 1 p. 21 - 22
反应条件
fluorine in formic acid
T=0.6°C; 1 h;
参考文献
Chambers, Richard D.; Hutchinson, John; Batsanov, Andrei S.; Lehmann, Christian W.; Naumov, Dimitrii Y.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2271 - 2275
反应条件
1: 77 percent / Ag2CO3, celite / acetonitrile
2: NaIO4 / methanol; H2O / 24 h / Ambient temperature
3: pyridine / CCl4 / 2 h / Heating
View Scheme
参考文献
Lee Yong Rok, R.; Kim, Nam Suk; Kim, Byung So
Tetrahedron Letters, 1997 , vol. 38, # 32 p. 5671 - 5674
反应条件
sulfuric acid; sodium hydrogencarbonate
1) CHCl3, r.t., 2) r.t.; Yield given. Multistep reaction;
参考文献
Ogino, Takashi; Kurihara, Chihiro; Baba, Yoshiyasu; Kanematsu, Ken
Journal of the Chemical Society, Chemical Communications, 1994 , # 17 p. 1979 - 1980
反应条件
in formic acid
1 h; Heating;
参考文献
Jurd, Leonard
Australian Journal of Chemistry, 1980 , vol. 33, # 8 p. 1603 - 1610
