5,5-二甲基-1,3-环己二酮合成路线 (共 504 条)
反应条件
in dichloromethane
T=20°C; 15 h; Inert atmosphere;
参考文献
Grieco, Liane M.; Halliday, Gary A.; Junk, Christopher P.; Lustig, Steven R.; Marshall, William J.; Petrov, Viacheslav A.
Journal of Fluorine Chemistry, 2011 , vol. 132, # 12 p. 1198 - 1206
反应条件
(NH4)2CO3 in water
T=20°C; 1 h; Green chemistry;
参考文献
Ray, Suman; Brown, Mike; Bhaumik, Asim; Dutta, Arghya; Mukhopadhyay, Chhanda
Green Chemistry, 2013 , vol. 15, # 7 p. 1910 - 1924
反应条件
potassium hydroxide in ethanol
0.25 h;
参考文献
Vovk; Chubaruk; Bol'but
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 2 p. 280 - 281
反应条件
4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane
T=20°C; 3 h; Inert atmosphere;
参考文献
Kim, Jonghoon; Song, Heebum; Park, Seung Bum
European Journal of Organic Chemistry, 2010 , # 20 p. 3815 - 3822
反应条件
pyridine in chloroform
参考文献
Akhrem,A.A. et al.
Synthesis, 1978 , p. 925 - 927
反应条件
1: benzene
3: sodium methylate; methanol
View Scheme
参考文献
Leonard; Adamcik
Journal of the American Chemical Society, 1959 , vol. 81, p. 595,599
反应条件
potassium carbonate in dimethyl sulfoxide
10 h; Ambient temperature;
参考文献
Zefirov, N. S.; Kuznetsova, T. S.; Kozhushkov, S. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 8 p. 1412 - 1415
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1599 - 1602
反应条件
silica-supported phosphorous pentoxide
T=80°C; 0.0833333 h; Neat (no solvent); chemoselective reaction;
参考文献
Mohammadizadeh, Mohammad R.; Hasaninejad; Bahramzadeh; Khanjarlou, Z. Sardari
Synthetic Communications, 2009 , vol. 39, # 7 p. 1152 - 1165
参考文献
Nemeryuk, M. P.; Tolokontseva, L. A.; Yadrovskaya, V. A.; Polezhaeva, A. I.; Petrova, G. A.; et al.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 7 p. 459 - 462
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 7 p. 810 - 814
反应条件
ammonium acetate in water
0.666667 h; Reflux;
参考文献
Xia, Jing-Jing; Zhang, Ke-Hua
Molecules, 2012 , vol. 17, # 5 p. 5339 - 5345