5,5-二甲基-1,3-环己二酮合成路线 (共 504 条)
反应条件
1: 53 percent / Et3N / methanol / 12 h / Heating
2: P2O5 / acetic acid / 1 h / Heating
View Scheme
参考文献
Ahluwalia, V K; Kiran, Sushma; Aggarwal, R; Arora, K K
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 12 p. 1095 - 1097
反应条件
H3[PW12O40]
T=90°C; Biginelli Pyrimidone Synthesis; 4 h; Ionic liquidSchlenk technique;
参考文献
Alvim, Haline G. O.; De Lima, Tatiani B.; De Oliveira, Heibbe C. B.; Gozzo, Fabio C.; De MacEdo, Julio L.; Abdelnur, Patricia V.; Silva, Wender A.; Neto, Brenno A. D.
ACS Catalysis, 2013 , vol. 3, # 7 p. 1420 - 1430
反应条件
DPAT in ethanol
Pseudo Biginelli like reaction; 5 h; Reflux;
参考文献
Li, Jianjun; Sun, Jian; Su, Weike
Letters in Organic Chemistry, 2010 , vol. 7, # 4 p. 314 - 318
参考文献
Desai
Journal of the Chemical Society, 1943 , p. 1079,1081
反应条件
in 1,2-dichloro-ethane
24 h; Heating;
参考文献
Coates, Robert M.; Hobbs, Steven J.
Journal of Organic Chemistry, 1984 , vol. 49, p. 140 - 152
反应条件
potassium carbonate in dimethyl sulfoxide
10 h; Ambient temperature;
参考文献
Zefirov, N. S.; Kuznetsova, T. S.; Kozhushkov, S. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 8 p. 1412 - 1415
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1599 - 1602
反应条件
potassium carbonate in dimethyl sulfoxide
10 h; Ambient temperature;
参考文献
Zefirov, N. S.; Kuznetsova, T. S.; Kozhushkov, S. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 8 p. 1412 - 1415
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1599 - 1602
反应条件
potassium carbonate in dimethyl sulfoxide
10 h; Ambient temperature;
参考文献
Zefirov, N. S.; Kuznetsova, T. S.; Kozhushkov, S. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 8 p. 1412 - 1415
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1599 - 1602
反应条件
potassium carbonate in dimethyl sulfoxide
10 h; Ambient temperature;
参考文献
Zefirov, N. S.; Kuznetsova, T. S.; Kozhushkov, S. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 8 p. 1412 - 1415
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1599 - 1602
反应条件
potassium carbonate in dimethyl sulfoxide
10 h; Ambient temperature;
参考文献
Zefirov, N. S.; Kuznetsova, T. S.; Kozhushkov, S. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 8 p. 1412 - 1415
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 8 p. 1599 - 1602