5,5-二甲基-1,3-环己二酮合成路线 （共 504 条）
反应条件
in water; N,N-dimethyl-formamide
T=100°C; Yield given;
参考文献
Tada, Masahiro; Takakuwa, Takako; Nagai, Masashi; Yoshii, Takao
Agricultural and Biological Chemistry, 1990 , vol. 54, # 11 p. 3061 - 3063
参考文献
Bakibaev, A. A.; Filimonov, V. D.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 4 p. 736 - 740
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 4 p. 854 - 859
参考文献
Akhrem, A. A.; Pshenichnyi, V. N.; Gulyakevich, O. V.; Khripach, V. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 8 p. 947
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 8 p. 1130 - 1131
反应条件
boron trifluoride diethyl etherate in benzene
6 h; Heating;
参考文献
Azzaro, Marcel; Geribaldi, Serge; Videau, Bruno
Synthesis, 1981 , # 11 p. 880 - 881
参考文献
Haas
Journal of the Chemical Society, 1909 , vol. 95, p. 424
反应条件
1: 91 percent / 1 h / Heating
2: 64 percent / butan-1-ol; acetic acid / 2 h / Heating
View Scheme
参考文献
Gautam, Poonam; Chaudhary, Ram P.
Journal of Chemical Research, 2014 , vol. 38, # 4 p. 226 - 230
参考文献
Ionescu; Georgescu
Bulletin de la Societe Chimique de France, 1929 , vol. <4> 45, p. 432
反应条件
1: H2, AcOH / PtO2
2: ZnCl2, aq. HCl
3: (i) Mg, MeI, Et2O, (ii) /BRN= 1900390/
4: (i) SOCl2, (ii) /BRN= 605631/, Et2O
5: (i) PCl5, benzene, (ii) /BRN= 2206155/, Li, Et2O
View Scheme
参考文献
Smissman,E.E.; Diebold,J.L.
Journal of Organic Chemistry, 1965 , vol. 30, p. 4002 - 4005
反应条件
Montmorillonite K 10; toluene-4-sulfonic acid
T=20°C; 24 h;
参考文献
Mansilla, Horacio; Afonso, Maria M.
Synthetic Communications, 2008 , vol. 38, # 15 p. 2607 - 2618
反应条件
T=60 - 70°C; Inert atmosphere;
参考文献
ELKIMIA; ABOU-KHALIL, Elie; RAEPPEL, Stéphane; RAEPPEL, Franck
Patent: WO2013/181741 A1, 2013 ;
Location in patent: Page/Page column 41 ;
