5,5-二甲基-1,3-环己二酮合成路线 （共 504 条）
参考文献
Gautam, Poonam; Chaudhary, Ram P.
Journal of Chemical Research, 2014 , vol. 38, # 4 p. 226 - 230
反应条件
triethylamine in methanol
12 h; Heating;
参考文献
Ahluwalia, V K; Kiran, Sushma; Aggarwal, R; Arora, K K
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 12 p. 1095 - 1097
参考文献
Ye, Yang; Wang, Linfei; Fan, Renhua
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1760 - 1763
反应条件
ammonium nitrate; bentonite in N,N-dimethyl-formamide
0.0833333 h; Irradiation;
参考文献
Cotterill, Ian C.; Usyatinsky, Alexander Ya.; Arnold, John M.; Clark, Douglas S.; Dordick, Jonathan S.; Michels, Peter C.; Khmelnitsky, Yuri L.
Tetrahedron Letters, 1998 , vol. 39, # 10 p. 1117 - 1120
反应条件
triphenylphosphine diiodide; triethylamine in acetonitrile
96 h; Ambient temperature;
参考文献
Piers, Edward; Grierson, John R.; Lau, Cheuk Kun; Nagakura, Isao
Canadian Journal of Chemistry, 1982 , vol. 60, p. 210 - 223
反应条件
1.1: NaH / tetrahydrofuran / 0 °C
1.2: tetrahydrofuran / 6 h / 20 °C
2.1: 91 percent / tellurium / tetrahydrofuran; hexane / 0.33 h / 0 °C
3.1: CuCN / tetrahydrofuran / 0.33 h / -78 °C
3.2: 85 percent / tetrahydrofuran / 20 °C
View Scheme
参考文献
Zhou, Yong Fan; Huang, Nai Zheng
Synthetic Communications, 1982 , vol. 12, # 10 p. 795 - 800
反应条件
1: 89 percent / acetonitrile / 3 h / 20 °C
2: 95 percent / CH2Cl2 / 20 h / Heating
3: 82 percent / aq. KH2PO4 / CH2Cl2 / 4 h / 20 °C
View Scheme
参考文献
Weidner, Juergen; Vilsmaier, Elmar
Monatshefte fuer Chemie, 1987 , vol. 118, p. 1057 - 1072
参考文献
Mead Johnson and Company
Patent: US3998879 A1, 1976 ;
反应条件
1: 70 percent / potassium carbonate / CHCl3 / 48 h / 20 °C
2: 70 percent / acetic acid / 12 h / Heating
View Scheme
参考文献
Gonzalez-Chavez, Rodolfo; Martinez, Roberto; Torre-Bouscoulet, Maria Eugenia; Gallo, Marco; Gonzalez-Chavez, Marco Martin
Chemical and Pharmaceutical Bulletin, 2014 , vol. 62, # 1 p. 16 - 24
反应条件
C28H41O4P; sodium sulfate in toluene
T=60°C; Inert atmosphere; regioselective reaction;
参考文献
Moreau, Julie; Hubert, Claudie; Batany, Jessika; Toupet, Loic; Roisnel, Thierry; Hurvois, Jean-Pierre; Renaudz, Jean-Luc
Journal of Organic Chemistry, 2009 , vol. 74, # 23 p. 8963 - 8973
