5,5-二甲基-1,3-环己二酮合成路线 （共 504 条）
反应条件
1: K2CO3 / CHCl3
2: ethanol
View Scheme
参考文献
Nagarajan; David; Shah
Journal of Medicinal Chemistry, 1976 , vol. 19, # 4 p. 508 - 511
反应条件
1: K2CO3 / CHCl3
2: ethanol
View Scheme
参考文献
Nagarajan; David; Shah
Journal of Medicinal Chemistry, 1976 , vol. 19, # 4 p. 508 - 511
反应条件
1: 82.5 percent / p-CH3C6H4SO3H / benzene / Heating
2: 91 percent / LiAlH4
3: 91 percent / LiAlH4
4: 81 percent / propionic acid / 36 h / 138 °C
5: 95 percent / H2 / 10percent Pd/C / ethanol
6: LiAlH4
7: 76 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 2 h
View Scheme
参考文献
Wawrzenczyk, Czeslaw; Lochynski, Stanislaw
Monatshefte fuer Chemie, 1985 , vol. 116, p. 99 - 110
反应条件
triethylamine
T=160°C; 0.25 h;
参考文献
Zhuo, Jin-Cong; Schenk, Kurt
Helvetica Chimica Acta, 2002 , vol. 85, # 5 p. 1276 - 1283
反应条件
silica sulfuric acid in acetonitrile
0.0166667 h; Microwave irradiation;
参考文献
Datta, Bandita; Reddy, M. B. Madhusudana; Pasha
Synthetic Communications, 2011 , vol. 41, # 15 p. 2331 - 2336
反应条件
toluene-4-sulfonic acid in benzene
6 h; Reflux;
参考文献
Winska, Katarzyna; Grudniewska, Aleksandra; Chojnacka, Anna; Bialonska, Agata; Wawrzenczyk, Czeslaw
Tetrahedron Asymmetry, 2010 , vol. 21, # 6 p. 670 - 678
参考文献
Hayasi,Y. et al.
Bulletin of the Chemical Society of Japan, 1970 , vol. 43, p. 2506 - 2511
反应条件
triethylamine in pyridine
2 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Music, Irena; Golobic, Amalija; Vercek, Bojan
Heterocycles, 1998 , vol. 48, # 2 p. 353 - 358
参考文献
Desai
Journal of the Chemical Society, 1932 , p. 1079,1086
Full Text Show Details
Voitila <Fjaeder>
Annales Academiae Scientiarum Fennicae, Series A, 1937 , vol. 49, # 1 p. 18,68
参考文献
Desai
Journal of the Chemical Society, 1932 , p. 1079,1086
Full Text Show Details
Voitila <Fjaeder>
Annales Academiae Scientiarum Fennicae, Series A, 1937 , vol. 49, # 1 p. 18,68
