5,5-二甲基-1,3-环己二酮合成路线 （共 504 条）
反应条件
diethyl ether; mixture of gaseous nitrogen oxides
参考文献
Haas
Journal of the Chemical Society, 1907 , vol. 91, p. 1437
反应条件
in toluene
Heating / refluxdean-stark trap;
参考文献
Nardi, Monica; Cozza, Annalisa; Denino, Antonio; Oliverio, Manuela; Procopio, Antonio
Synthesis, 2012 , vol. 44, # 5 p. 800 - 804
反应条件
1: 3-nitro-aniline With hydrogenchloride; sodium nitrite in water
2: dimedone With sodium acetate in water
T=25°C; 4 h;
参考文献
Sethukumar; Arul Prakasam
Journal of Molecular Structure, 2010 , vol. 963, # 2-3 p. 250 - 257
参考文献
Gudrinieze et al.
Latvijas PSR Zinatnu Akademijas Vestis, 1959 , # 9 p. 101,103
Chem. Zentralbl., 1961 , vol. 132, p. 18672
反应条件
1: 4-bromo-aniline With hydrogenchloride; sodium hydroxide; sodium nitrite in water
T=0 - 5°C; 1 h;
2: dimedone With sodium hydroxide in water
Japp-Klingemann reaction; 1 h; Cooling with ice;
参考文献
Mahmudov, Kamran T.; Maharramov, Abel M.; Aliyeva, Rafiga A.; Chyragov, Famil M.; Askerov, Rizvan K.; Hasanov, Parvin Q.; Kopylovich, Maximilian N.; Pombeiro, Armando J.L.
Journal of Molecular Structure, 2011 , vol. 1006, # 1-3 p. 576 - 579
反应条件
N-sulfonic acid poly(4-vinylpyridinium) chloride
T=100°C; 0.133333 h;
参考文献
Shirini, Frahad; Abedini, Masoumeh; Pourhasan, Reyhaneh
Dyes and Pigments, 2013 , vol. 99, # 1 p. 250 - 255
反应条件
iodine; zinc in methanol
T=70°C;
参考文献
Rong, Liangce; Li, Xiaoyue; Wang, Haiying; Shi, Daqing; Tu, Shujiang; Zhuang, Qiya
Synthetic Communications, 2006 , vol. 36, # 16 p. 2345 - 2353
反应条件
1: aqueous ethanol; piperidine
2: aq.-ethanolic hydrochloric acid
View Scheme
参考文献
Horning; Horning
Journal of Organic Chemistry, 1946 , vol. 11, p. 95,97, 98
反应条件
tetra-n-butylammonium acetate
T=100°C;
参考文献
Riyaz, Sd.; Indrasena; Naidu; Dubey
Synthetic Communications, 2014 , vol. 44, # 3 p. 368 - 373
参考文献
Gudrinieze et al.
Latvijas PSR Zinatnu Akademijas Vestis, 1959 , # 9 p. 101,103
Chem. Zentralbl., 1961 , vol. 132, p. 18672
