2-氯-1.3-丁二烯合成路线 （共 128 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=20°C; 48 h; Product distribution;
参考文献
Cottrell; Golding; Munter; Watson
Chemical Research in Toxicology, 2001 , vol. 14, # 11 p. 1552 - 1562
反应条件
in xylene; benzene
4 h; Heating;
参考文献
Kimura, Yoshikazu; Suzuki, Michiyo; Matsumoto, Teruyo; Abe, Rumiko; Terashima, Shiro
Chemistry Letters, 1984 , p. 473 - 476
Title/Abstract Show Details
Kimura; Suzuki; Matsumoto; et al.
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 2 p. 415 - 421
反应条件
dilithium tetrachlorocuprate; magnesium; ethylene dibromide; zinc(II) chloride
1.) THF, reflux, 3 h, 2.) THF, Et2O, RT, overnight; Yield given. Multistep reaction;
参考文献
Shea, Kenneth J.; Kim, Jang-Seob
Journal of the American Chemical Society, 1992 , vol. 114, # 8 p. 3044 - 3051
反应条件
dilithium tetrachlorocuprate; magnesium; ethylene dibromide; zinc(II) chloride
1.) THF, reflux, 3 h, 2.) THF, Et2O, RT, overnight; Yield given. Multistep reaction;
参考文献
Shea, Kenneth J.; Kim, Jang-Seob
Journal of the American Chemical Society, 1992 , vol. 114, # 8 p. 3044 - 3051
反应条件
triethylamine; hydroquinone in benzene
T=40°C; 24 h; Yield given. Title compound not separated from byproducts;
参考文献
Fliege, Werner; Huisgen, Rolf; Kolbeck, Winfried; Weberndoerfer, Volkmar
Chemische Berichte, 1983 , vol. 116, # 10 p. 3438 - 3460
反应条件
triethylamine; hydroquinone in benzene
T=40°C; 24 h; Yield given. Title compound not separated from byproducts;
参考文献
Fliege, Werner; Huisgen, Rolf; Kolbeck, Winfried; Weberndoerfer, Volkmar
Chemische Berichte, 1983 , vol. 116, # 10 p. 3438 - 3460
反应条件
hydroquinone; acetone
参考文献
Furdik et al.
Chemicke Zvesti, 1959 , vol. 13, p. 581,583, 584
Chem.Abstr., 1960 , p. 7963
参考文献
Zubritskii, L. M.; Romashchenkova, N. D.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2157 - 2167
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2465 - 2477
反应条件
ozone
T=-78°C; Further byproducts given;
参考文献
Griesbaum, Karl; Meister, Martin
Chemische Berichte, 1987 , vol. 120, p. 1573 - 1580
反应条件
ozone
T=-78°C; Further byproducts given. Yields of byproduct given;
参考文献
Griesbaum, Karl; Meister, Martin
Chemische Berichte, 1987 , vol. 120, p. 1573 - 1580
