7-氨基-3-(2-溴乙氧基)-4-氯异苯并吡喃-1-酮合成路线 （共 4 条）
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran T=20°C; 6 h; atmospheric pressure;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 14 p. 3141 - 3152
反应条件
1: 73 percent / H2SO4 / 0.12 h / 70 °C 2: 44 percent / PCl5 / toluene / 15 h / Heating 3: 100 percent / H2 / Pd/C / tetrahydrofuran / 6 h / 20 °C / atmospheric pressure View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 14 p. 3141 - 3152
反应条件
1: 44 percent / PCl5 / toluene / 15 h / Heating 2: 100 percent / H2 / Pd/C / tetrahydrofuran / 6 h / 20 °C / atmospheric pressure View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 14 p. 3141 - 3152
反应条件
1: 88 percent / nitric acid / 6 h / 20 °C 2: 73 percent / H2SO4 / 0.12 h / 70 °C 3: 44 percent / PCl5 / toluene / 15 h / Heating 4: 100 percent / H2 / Pd/C / tetrahydrofuran / 6 h / 20 °C / atmospheric pressure View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 14 p. 3141 - 3152
