1: bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); dtbpy / tetrahydrofuran / 24 h / 80 °C / |High pressure; |Inert atmosphere 2: 1,10-phenanthroline; copper(l) iodide; potassium iodide / methanol; water / 1 h / 80 °C / |High pressure View Scheme