反应条件
1: With triethylamine; 4H-1,2,4-triazole; trichlorophosphate in acetonitrile
T=-20 - 0°C; 2 h;
2: With water in acetonitrile
T=10°C;
3: With ammonia in 1,4-dioxane; water
参考文献
Monia, Brett P.; Freier, Susan M.; Manoharan, Muthiah; Gaarde, William A.; Griffey, Richard H.; Swayze, Eric E.; Bennett, C. Frank
Patent: US2005/130924 A1, 2005 ;
Location in patent: Page/Page column 16; 17 ;