反应条件
1: (ethyl)-triphenylphosphonium bromide With potassium 2-methyl-2-butoxide in tetrahydrofuran; toluene
Wittig Olefination; 0.333333 h; Inert atmosphereSchlenk technique;
2: C7H4INO3 in tetrahydrofuran; toluene
T=0°C; 1.25 h; Inert atmosphereSchlenk technique; Overall yield = 65 percent; Overall yield = 0.751 g;
参考文献
Barbasiewicz, Michal; Malinska, Maura; Blocki, Krzysztof
Journal of Organometallic Chemistry, 2013 , vol. 745-746, p. 8 - 11