(2-氨基-1-吡啶鎓基)乙酸酯合成路线 （共 11 条）
反应条件
triethylamine in water T=90°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 53, # 3 p. 297 - 300
参考文献
DE451733 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 15, p. 336
Chemische Berichte, , vol. 57, p. 1384
Chemische Berichte, , vol. 57, p. 2098
DE414146 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 15, p. 455
参考文献
DE451733 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 15, p. 336
Chemische Berichte, , vol. 57, p. 1384
Chemische Berichte, , vol. 57, p. 2098
DE414146 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 15, p. 455
反应条件
alkaline solution; water
参考文献
Kirpal; Wojnar
Chemische Berichte, 1938 , vol. 71, p. 1261,1265
反应条件
1: trichlorophosphate / toluene / 16 h / Reflux 2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethylene glycol dimethyl ether; water / 6 h / Inert atmosphere; Sealed vessel; Reflux View Scheme
参考文献
Bazin, Marc-Antoine; Marhadour, Sophie; Tonnerre, Alain; Marchand, Pascal
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5378 - 5382
反应条件
T=200 - 205°C; laengeres Erhitzen im Stickstoffstrom;
参考文献
Reindel; Rauch
Chemische Berichte, 1925 , vol. 58, p. 396
反应条件
T=200 - 205°C; laengeres Erhitzen im Stickstoffstrom;
参考文献
Reindel; Rauch
Chemische Berichte, 1925 , vol. 58, p. 396
反应条件
1: trichlorophosphate / toluene / 16 h / |Reflux
2: sulfuric acid; nitric acid / 3.5 h / -5 - 20 °C
View Scheme
参考文献
Bazin, Marc-Antoine; Marhadour, Sophie; Tonnerre, Alain; Marchand, Pascal
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5378 - 5382
反应条件
1: trichlorophosphate / toluene / 16 h / |Reflux
2: sulfuric acid; nitric acid / 3.5 h / -5 - 20 °C
3: 1-methyl-pyrrolidin-2-one / 96 h / 170 °C / |Sealed tube
View Scheme
参考文献
Bazin, Marc-Antoine; Marhadour, Sophie; Tonnerre, Alain; Marchand, Pascal
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5378 - 5382
反应条件
1: trichlorophosphate / toluene / 16 h / Reflux
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethylene glycol dimethyl ether; water / 6 h / Inert atmosphere; Sealed vessel; Reflux
3: N-bromosuccinmide / acetonitrile / 2 h / 20 °C
View Scheme
参考文献
Marhadour, Sophie; Bazin, Marc-Antoine; Marchand, Pascal
Tetrahedron Letters, 2012 , vol. 53, # 3 p. 297 - 300
