2,3-二氟吡啶-4-基硼酸合成路线 (共 2 条)
反应条件
1: 2,3-difluoropyridine With n-butyllithium; diisopropylamine in tetrahydrofuran; hexanes T=-78°C; 1.25 h; 2: tri-isopropoxy-borane in tetrahydrofuran; hexanes T=-78°C; 1 h;
参考文献
US2011/28492 A1, ;
Page/Page column 27 ;
反应条件
1: With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-78°C; 1 h; 2: With tri-isopropoxy-borane in tetrahydrofuran; hexane T=-78°C; 1 h;
参考文献
WO2012/101065 A2, ;
Page/Page column 138 ;
WO 2012/101065 A2