N-(2,3-二氢-5-甲基-2-氧代-4-嘧啶基)-苯甲酰胺合成路线 （共 6 条）
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile 7 h; Heating;
参考文献
Holy, Antonin; Rosenberg, Ivan; Dvorakova, Hana
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 8 p. 2190 - 2210
反应条件
1: 88 percent / NH3; water / 3 h / Heating 2: 76 percent / DMAP / acetonitrile / 7 h / Heating View Scheme
参考文献
Buchini, Sabrina; Leumann, Christian J.
European Journal of Organic Chemistry, 2006 , # 14 p. 3152 - 3168
反应条件
1.1: POCl3; Et3N / acetonitrile / 1.17 h / 0 - 20 °C 1.2: 59 percent / acetonitrile / 9 h 2.1: 88 percent / NH3; water / 3 h / Heating 3.1: 76 percent / DMAP / acetonitrile / 7 h / Heating View Scheme
参考文献
Buchini, Sabrina; Leumann, Christian J.
European Journal of Organic Chemistry, 2006 , # 14 p. 3152 - 3168
反应条件
1: NH3 / methanol / 1) With methanolic NH3 in autoclave at 120 deg C for 6 h 2: 78 percent / 4-Dimethylaminopyridine / acetonitrile / 7 h / Heating View Scheme
参考文献
Holy, Antonin; Rosenberg, Ivan; Dvorakova, Hana
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 8 p. 2190 - 2210
反应条件
1: 2 h / Heating 2: trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 0.08 h / Ambient temperature 3: 95 percent / Bu4NF / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Chanteloup, Luc; Thuong, Nguyen T.
Tetrahedron Letters, 1994 , vol. 35, # 6 p. 877 - 880
反应条件
1: 2 h / Heating
2: trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 0.08 h / Ambient temperature
3: 95 percent / Bu4NF / tetrahydrofuran / Ambient temperature
4: 88 percent / pyridine / Ambient temperature
View Scheme
参考文献
Chanteloup, Luc; Thuong, Nguyen T.
Tetrahedron Letters, 1994 , vol. 35, # 6 p. 877 - 880
