反应条件
1.1: 4-(N,N-dimethlyamino)pyridine / pyridine / 24 h / 20 °C 2.1: acetic anhydride; dimethyl sulfoxide / 2 h / 50 °C 3.1: toluene / 4 h / -40 °C 4.1: magnesium / methanol / 2 h / 20 °C 5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C 6.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C 6.2: 0 - 20 °C 7.1: pyridine / dichloromethane / 2 h / 0 °C 8.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C 9.1: dichloromethane / 1 h / 0 °C 10.1: sodium carbonate / tert-butyl benzene / 24 h / 170 °C 11.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C 12.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C 13.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C 14.1: scandium tris(trifluoromethanesulfonate) / dichloromethane; water / 20 - 40 °C 15.1: Jone's reagent / water; acetone / 0 - 20 °C 16.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 20 °C 17.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C 18.1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 20 - 60 °C 19.1: pyridine; sodium periodate; osmium(VIII) oxide / water; tert-butyl alcohol / 20 - 50 °C 20.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C 20.2: 0.33 h / -78 °C 20.3: 6 h / -78 °C 21.1: boron trichloride / n-heptane; dichloromethane / 0.67 h / 0 °C 22.1: water / n-heptane; dichloromethane / 0.33 h / 0 °C 23.1: BOPCl / dichloromethane / 2 h / 20 °C 24.1: dichlorotriphenylphosphorane / pyridine; acetonitrile / 3 h / 20 °C View Scheme
参考文献
Kaiya, Yuji; Hasegawa, Jun-Ichi; Momose, Takayuki; Sato, Takaaki; Chida, Noritaka
Chemistry - An Asian Journal, 2011 , vol. 6, # 1 p. 209 - 219
