反应条件
With t-butyl lithium; hydrochloric acid; LiAlH4 in diethyl ether; pentane byproducts: LiCl; reaction of mesityltrichlorogermane and tert-butyllithium in soln. at 0°C, warming to room temp., elimination of LiCl, redn. of the crude product with LiAlH4 in diethyl ether, refluxing for 3 h, hydrolysis with HCl; extn. with pentane, drying on Na2SO4, distn., elem. anal.;
参考文献
Ranaivonjatovo, Henri; Escudie, Jean; Couret, Claude; Satge, Jacques New Journal of Chemistry, 1989 , vol. 13, p. 389 - 398