N,N,N-trimethylbenzenemethanaminium dichloroiodate in tetrahydrofuran Ambient temperature;

1: 70 percent / K2CO3, tetrabutylammonium bromide / butan-2-one / 12 h / 60 °C 2: 75 percent / benzyltrimethylammonium dichloroiodate / tetrahydrofuran / Ambient temperature View Scheme

trichlorophosphate 1.) room temp., 6 h, 2.) 1,2-dichloroethane, room temp., 16 h; Yield given. Multistep reaction. Yields of byproduct given;

trichlorophosphate 1.) room temp., 6 h, 2.) 1,2-dichloroethane, room temp., 16 h; Yield given. Multistep reaction. Yields of byproduct given;