1: With tert.-butyl lithium in diethyl ether; pentane T=-40 - -20°C; 8 h; Inert atmosphere; 2: With 1,2-dibromo-1,1,2,2-tetrachloroethane in diethyl ether; pentane T=0 - 25°C; 12 h; 3: With hydrogenchloride; water in diethyl ether; pentane T=0°C; 1 h;
参考文献
THE TRUSTEES OF COLUMBIA UNIVERSITY IN THE CITY OF NEW YORK; SNYDER, Scott Alan; SHERWOOD, Trevor C.; ROSS, Audrey G.; OH, Hyunju; GHOSH, Sankar
Patent: WO2011/103442 A2, 2011 ;
Location in patent: Page/Page column 72-73 ;
