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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氰基苯硼酸
合成路线
（共 139 条）
126747-14-6
4-氰基苯硼酸
→
反应条件
67856-50-2
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / tetrahydrofuran; water / 20 - 80 °C / |Schlenk technique; |Inert atmosphere 2: sodium hydroxide; water / tetrahydrofuran / 80 °C View Scheme
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
15155-41-6
4,7-二溴-2,1,3-苯并噻二唑
+
126747-14-6
4-氰基苯硼酸
→
反应条件
867349-78-8
反应条件
cesium fluoride in 1,4-dioxane Suzuki coupling reaction;
参考文献
DaSilveira Neto, Brenno A.; Lopes, Aline S.; Wuest, Martina; Costa, Valentim E. U.; Ebeling, Guenter; Dupont, Jairton
Tetrahedron Letters, 2005 , vol. 46, # 40 p. 6843 - 6846
924-44-7
乙醛酸乙酯
+
126747-14-6
4-氰基苯硼酸
→
反应条件
847227-46-7
4-氰基扁桃酸乙酯
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate; biphenyl-2-yl-di-tert-butyl-phosphane in toluene T=80°C; Suzuki-Miyaura coupling reaction; 23 h; Inert atmosphere;
参考文献
Francesco, Irene Notar; Wagner, Alain; Colobert, Francoise
European Journal of Organic Chemistry, 2008 , # 34 p. 5692 - 5695
884494-53-5
2-氯-3-溴-4-碘吡啶
+
126747-14-6
4-氰基苯硼酸
→
反应条件
917969-36-9
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; toluene T=100°C; 36 h;
参考文献
Sun, Chongqing; Sher, Philip M.; Wu, Gang; Ewing, William R.; Huang, Yanting; Lee, Taekyu; Murugesan, Natesan; Sulsky, Richard B.
Patent: US2007/4772 A1, 2007 ;
Location in patent: Page/Page column 34 ;
126747-14-6
4-氰基苯硼酸
→
反应条件
94268-29-8
反应条件
1.1: trans-2-aminocyclohexanol hydrochloride; NiI2; sodium hexamethyldisilazane / isopropyl alcohol / 0.17 h / 20 °C / |Inert atmosphere 1.2: 1 h / 80 °C 2.1: hydrogenchloride / 1,4-dioxane / 1.5 h / 20 °C View Scheme
参考文献
3-V BIOSCIENCES, INC.; OSLOB, Johan D.; MCDOWELL, Robert S.; JOHNSON, Russell; YANG, Hanbiao; EVANCHIK, Marc; ZAHARIA, Cristiana A.; CAI, Haiying; HU, Lily W.
Patent: WO2014/8197 A1, 2014 ;
1666-13-3
二苯基二硒醚
+
126747-14-6
4-氰基苯硼酸
→
反应条件
94800-52-9
反应条件
sodium tetrahydroborate; 1,10-phenanthroline; CuSO4‵5H2O in ethanol T=20°C; 8 h;
参考文献
Kumar, Amit; Kumar, Sangit
Tetrahedron, 2014 , vol. 70, # 9 p. 1763 - 1772
126747-14-6
4-氰基苯硼酸
+
460748-15-6
→
反应条件
460746-48-9
4-[2-(2-羟基乙基)-1-苯并呋喃-5-基]苯甲腈
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0); 2-dicyclohexylphosphino-1,1'-biphenyl in ethylene glycol dimethyl ether; water T=80°C;
参考文献
Cowart, Marlon D.; Pu, Yu-Ming; Ku, Yi-Yin; Grieme, Timothy A.; Gupta, Ashok K.; Plata, Daniel J.; Faghih, Ramin; Gfesser, Gregory A.
Patent: US2004/54185 A1, 2004 ;
Location in patent: Page 12 ;
US 20040054185 A1
60577-30-2
+
126747-14-6
4-氰基苯硼酸
→
反应条件
460748-08-7
4-羟基-3-甲基-[1,1-联苯]-4-甲腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tripotassium phosphate monohydrate in water; isopropyl alcohol T=70°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Jensen, Thomas Binderup; Terazzi, Emmanuel; Buchwalder, Kerry-Lee; Guenee, Laure; Nozary, Homayoun; Schenk, Kurt; Heinrich, Benoit; Donnio, Bertrand; Guillon, Daniel; Piguet, Claude
Inorganic Chemistry, 2010 , vol. 49, # 18 p. 8601 - 8619
2362-12-1
+
126747-14-6
4-氰基苯硼酸
→
反应条件
460748-08-7
4-羟基-3-甲基-[1,1-联苯]-4-甲腈
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate in water; isopropyl alcohol T=70°C; Suzuki-Miyaura Coupling; 15 h; Inert atmosphere;
参考文献
Dutronc, Thibault; Terazzi, Emmanuel; Guenee, Laure; Buchwalder, Kerry-Lee; Spoerri, Aurore; Emery, Daniel; Mareda, Jiri; Floquet, Sebastien; Piguet, Claude
Chemistry - A European Journal, 2013 , vol. 19, # 26 p. 8447 - 8456
4559-70-0
二苯基磷氧
+
126747-14-6
4-氰基苯硼酸
→
反应条件
5032-54-2
反应条件
palladium diacetate; sodium carbonate; 1,4-di(diphenylphosphino)-butane in 1,4-dioxane T=90°C; 24 h; Green chemistry;
参考文献
Fu, Tingting; Qiao, Hongwei; Peng, Zhimin; Hu, Gaobo; Wu, Xueji; Gao, Yuxing; Zhao, Yufen
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 18 p. 2895 - 2902
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