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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
126784-41-6
合成路线
（共 10 条）
113709-48-1
→
反应条件
126784-41-6
反应条件
hydrogen; palladium in ethyl acetate P=760 Torr; 12 h;
参考文献
Ferraboschi, Patrizia; Grisenti, Paride; Manzocchi, Ada; Santaniello, Enzo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 9 p. 1159 - 1162
130614-61-8
→
反应条件
126784-41-6
反应条件
hydrogen; palladium on activated charcoal in diethyl ether 10 h;
参考文献
Wallace, Paul A.; Minnikin, David E.; McCrudden, Katharine; Pizzarello, Andrea
Chemistry and Physics of Lipids, 1994 , vol. 71, # 2 p. 145 - 162
98061-08-6
→
反应条件
126784-41-6
反应条件
lithium chloride in water; dimethyl sulfoxide 6 h; Heating;
参考文献
Shimamura, Hiroyuki; Sunazuka, Toshiaki; Izuhara, Takashi; Hirose, Tomoyasu; Shiomi, Kazuro; Omura, Satoshi
Organic Letters, 2007 , vol. 9, # 1 p. 65 - 67
124-13-0
正辛醛
→
反应条件
126784-41-6
反应条件
1: 91 percent / CH2Cl2 / 16 h / Ambient temperature 2: 88 percent / H2 / 10percent Pd/C / diethyl ether / 10 h View Scheme
参考文献
Wallace, Paul A.; Minnikin, David E.; McCrudden, Katharine; Pizzarello, Andrea
Chemistry and Physics of Lipids, 1994 , vol. 71, # 2 p. 145 - 162
629-27-6
1-碘辛烷
→
反应条件
126784-41-6
反应条件
1.1: NaH / dimethylformamide / 0.5 h / 0 °C 1.2: 99 percent / dimethylformamide / 0 - 20 °C 2.1: 86 percent / lithium chloride / H2O; dimethylsulfoxide / 6 h / Heating View Scheme
参考文献
Shimamura, Hiroyuki; Sunazuka, Toshiaki; Izuhara, Takashi; Hirose, Tomoyasu; Shiomi, Kazuro; Omura, Satoshi
Organic Letters, 2007 , vol. 9, # 1 p. 65 - 67
609-08-5
甲基丙二酸二乙酯
→
反应条件
126784-41-6
反应条件
1.1: NaH / dimethylformamide / 0.5 h / 0 °C 1.2: 99 percent / dimethylformamide / 0 - 20 °C 2.1: 86 percent / lithium chloride / H2O; dimethylsulfoxide / 6 h / Heating View Scheme
参考文献
Shimamura, Hiroyuki; Sunazuka, Toshiaki; Izuhara, Takashi; Hirose, Tomoyasu; Shiomi, Kazuro; Omura, Satoshi
Organic Letters, 2007 , vol. 9, # 1 p. 65 - 67
64-17-5
乙醇
+
24323-23-7
2-甲基癸酸
→
反应条件
126784-41-6
反应条件
sulfuric acid; toluene
参考文献
Voerde, Carin; Hoegberg, Hans-Erik; Hedenstroem, Erik
Tetrahedron Asymmetry, 1996 , vol. 7, # 5 p. 1507 - 1513
126784-41-6
→
反应条件
18675-24-6
2-甲基-1-癸醇
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 0.75 h;
参考文献
Shimamura, Hiroyuki; Sunazuka, Toshiaki; Izuhara, Takashi; Hirose, Tomoyasu; Shiomi, Kazuro; Omura, Satoshi
Organic Letters, 2007 , vol. 9, # 1 p. 65 - 67
126784-41-6
→
反应条件
19009-56-4
2-甲基癸醇
反应条件
1: 100 percent / LiAlH4 / tetrahydrofuran / 0.75 h / 0 °C 2: 100 percent / triethylamine; SO3*pyridine; DMSO / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Shimamura, Hiroyuki; Sunazuka, Toshiaki; Izuhara, Takashi; Hirose, Tomoyasu; Shiomi, Kazuro; Omura, Satoshi
Organic Letters, 2007 , vol. 9, # 1 p. 65 - 67
126784-41-6
→
反应条件
24323-23-7
2-甲基癸酸
反应条件
potassium hydroxide in methanol; toluene 24 h; Heating;
参考文献
Wallace, Paul A.; Minnikin, David E.; McCrudden, Katharine; Pizzarello, Andrea
Chemistry and Physics of Lipids, 1994 , vol. 71, # 2 p. 145 - 162
