反应条件
1: cyclohexyl-(2,2-dimethyl-[1,3]dioxan-5-ylidene)-amine With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-78 - -35°C; Inert atmosphere; 2: methyl iodide in tetrahydrofuran; hexane T=-78 - 25°C; 3 h; Inert atmosphere; 3: With water; ammonium chloride in tetrahydrofuran; hexane T=20°C;
参考文献
Behenna, Douglas C.; Mohr, Justin T.; Sherden, Nathaniel H.; Marinescu, Smaranda C.; Harned, Andrew M.; Tani, Kousuke; Seto, Masaki; Ma, Sandy; Novak, Zoltan; Krout, Michael R.; McFadden, Ryan M.; Roizen, Jennifer L.; Enquist Jr., John A.; White, David E.; Levine, Samantha R.; Petrova, Krastina V.; Iwashita, Akihiko; Virgil, Scott C.; Stoltz, Brian M.
Chemistry - A European Journal, 2011 , vol. 17, # 50 p. 14199 - 14223