4-(叔丁基二甲基锡氧基)-环己醇合成路线 （共 5 条）
反应条件
1H-imidazole in tetrahydrofuran; N,N-dimethyl-formamide T=0°C;
参考文献
Arora, Nidhi; Chen, Shaoqing; Hermann, Johannes Cornelius; Kuglstatter, Adreas; Labadie, Sharada Shenvi; Lin, Clara Jeou Jen; Lucas, Matthew C.; Moore, Amy Geraldine; Papp, Eva; Talamas, Francisco Xavier; Wanner, Jutta; Zhai, Yansheng
Patent: US2012/15962 A1, 2012 ;
Location in patent: Page/Page column 59 ;
US 20120015962 A1
反应条件
sodium tetrahydroborate in methanol T=-50 - 20°C;
参考文献
Zhuo, Jincong; Li, Yun-Long; Xu, Meizhong; He, Chunhong; Yao, Wenqing
Patent: US2007/208001 A1, 2007 ;
Location in patent: Page/Page column 50 ;
US 20070208001 A1
反应条件
methanol; samarium diiodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide Reflux; chemoselective reaction;
参考文献
Lam, Kevin; Marko, Istvan E.
Tetrahedron, 2009 , vol. 65, # 52 p. 10930 - 10940
反应条件
sodium hydride 1.) THF, 55 deg C, 18 h, 2.) THF, RT, 19 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
McDougal, Patrick G.; Rico, Joseph G.; Oh, Young-Im; Condon, Brian D.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3388 - 3390
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 6 h;
参考文献
Song, Zhen Lei; Wang, Bao Min; Tu, Yong Qiang; Fan, Chun An; Zhang, Shu Yu
Organic Letters, 2003 , vol. 5, # 13 p. 2319 - 2321
