反应条件
1.1: sulfuric acid / propan-1-ol; water / 20 h / Reflux 2.1: tetrahydrofuran; sodium tetrahydroborate; methyl iodide / 2 h / 10 - 20 °C / Inert atmosphere 2.2: 1 h / -10 - 29 °C / Inert atmosphere 2.3: immobilized lipase from Pseudomonas cepacia / 48 h / 20 °C / Inert atmosphere; Enzymatic reaction 3.1: methanol; potassium hydroxide / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere View Scheme
参考文献
Khachik, Frederick
Synthesis, 2012 , vol. 44, # 3 art. no. M102111SS, p. 453 - 459
