反应条件
1: SeO2, salicylic acid, tert-butyl hydroperoxide / CH2Cl2 / 27 h / Ambient temperature 2: PDC / CH2Cl2 / 10 h / Ambient temperature 3: 1.) n-BuLi / 1.) THF, -78 deg C, 2 h, 2.) THF, -78 deg C, 3 h 4: 94 percent / SOCl2, pyridine / benzene / 16 h / Ambient temperature 5: 91 percent / MeOK / toluene / 2 h / Ambient temperature 6: 1.) MeOK / 1.) cyclohexane, 38 deg C, 2 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 20 p. 3834 - 3838
