Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 11 p. 2414
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2598 - 2599
p-Nitro-benzoesaeure-fluorsulfonsaeureanhydrid in dichloromethane T=0°C; 14 h; further reagents: PhCOOSO2F, p-CH3-C6H4COOSO2F, p-Cl-C6H4COOSO2F; Title compound not separated from byproducts;
in neat (no solvent) soln. (liquid SO2) lost purple color within 15 min;; evapn. (SO2); identification of C6H6 and SO2(C6H5)2 by liquid chromy.; residue washed with benzene and dried; elem. anal. of unidentified Bi-compound;;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 11 p. 2414
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2598 - 2599
