2-苯基-3-丁炔-2-醇合成路线 （共 43 条）
反应条件
in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Gao, Yang; Wu, Wanqing; Huang, Huawen; Huang, Yubing; Jiang, Huanfeng
Chemical Communications, 2014 , vol. 50, # 7 p. 846 - 848
反应条件
1: acetylene With ethanol; potassium hydroxide semihydrate in dimethyl sulfoxide T=15°C; Favorskii Rearrangement; P=760.051 Torr; 0.5 h; 2: acetophenone in dimethyl sulfoxide 1 h;
参考文献
Shmidt; Bidusenko; Protsuk; Mikhaleva; Trofimov
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 1 p. 8 - 11
Zh. Org. Khim., 2013 , vol. 49, # 1 p. 18 - 21,4
反应条件
P(MeNCH2CH2)3N in methanol 41 h; Ambient temperature;
参考文献
Ilankumaran, Palanichamy; Verkade
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3086 - 3089
反应条件
methanol; potassium carbonate T=20°C; 12 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 2 p. 500 - 511
反应条件
1: in tetrahydrofuran T=-78 - -20°C; 2: With water; ammonium chloride in tetrahydrofuran
参考文献
Angewandte Chemie, International Edition, , vol. 48, p. 4528 - 4531
Angewandte Chemie, , vol. 121, p. 4598 - 4601
反应条件
1.1: n-butyllithium / tetrahydrofuran / 1.5 h / -70 °C / Inert atmosphere 1.2: 1.5 h / -70 - 20 °C / Inert atmosphere 1.3: 0 °C 2.1: methanol; potassium carbonate / 12 h / 20 °C / Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 2 p. 500 - 511
反应条件
acetylene in N,N-dimethyl acetamide; benzene T=35°C; 1.75 h;
参考文献
Journal of Organic Chemistry, , vol. 29, p. 1872 - 1876
参考文献
US2125384 , ;
Journal of the American Chemical Society, , vol. 60, p. 2882
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2062,2064
反应条件
potassium carbonate T=160 - 170°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 9, p. 396,399
Chem. Zentralbl., , vol. 110, # II p. 4464
