in tetrahydrofuran; toluene addn. of LiC5H5 in THF to Pd-complex in toluene, stirring (several h); solvent removal (vac.), sublimation (45°C, 1E-3 Torr);;
参考文献
Thomas; Park
Journal of the Electrochemical Society, 1989 , vol. 136, # 6 p. 1661 - 1666
in acetone dropwise addn. of the ligand to an acetone soln. of the staring complex at 0°C, stirring for 15 min at room temp.; filtn. of the solid, washing (acetone), drying in vac., elem. anal.;
Gubin, S. P.; Rubezhov, A. Z.; Winch, B. L.; Nesmeyanov, A. N.
Tetrahedron Letters, 1964 , p. 2881 - 2887
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Gmelin Handbook: Fe: Org.Verb.A1, 2.1.2.3, page 23 - 24
