反应条件
in tetrahydrofuran Irradiation (UV/VIS); exclusion of air and moisture; Ar, Schlenk-technique; soln. of As-Mo-complex and Ni compd. in THF is irradiated at -10°C for 4 h; evapn. in vac., addn. of CH2Cl2, chromy. (-15°C, silica gel) with hexane/CH2Cl2 1. Cp2Ni, 2. Cp2Ni2(CO)2, 3. AsCp3Mo2Ni(CO)4, 4. Cp3Ni3(CO)2, 5. AsCp3Mo3(CO)6, with THF As2Cp6Mo4Ni2(CO)7; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 429, # 2 p. 173 - 186
