triphenylphosphine in diethyl ether; toluene (CH3)2CCO in ether, Ni(C5H5)2 in toluene (in about molar ratio 3:1); room temp./2 d; drying, multiple recrystn. from n-hexane/C6H6; P(C6H5)3)2Ni(CO)2 is isolated from filtrate on effect of P(C6H5)3;
参考文献
Journal of Organometallic Chemistry, , vol. 26, p. 267 - 270
in n-heptane byproducts: CO; under Ar, refluxed for 1.5 h; detn. by IR-spectroscopy;
参考文献
Kaganovich, V. S.; Slovokhotov, Yu. L.; Mironov, A. V.; Struchkov, Yu. T.; Rybinskaya, M. I.
Journal of Organometallic Chemistry, 1989 , vol. 372, p. 339 - 350
Kaganovich, V. S.; Slovokhotov, Yu. L.; Mironov, A. V.; Struchkov, Yu. T.; Rybinskaya, M. I.
Journal of Organometallic Chemistry, 1989 , vol. 372, p. 339 - 350
in n-heptane byproducts: CO; under Ar, refluxed for 1.5 h; detn. by IR-spectroscopy;
参考文献
Kaganovich, V. S.; Slovokhotov, Yu. L.; Mironov, A. V.; Struchkov, Yu. T.; Rybinskaya, M. I.
Journal of Organometallic Chemistry, 1989 , vol. 372, p. 339 - 350
in toluene byproducts: CH4; under Ar or in a vac.; addn. of Cd-compd. to soln. of Ni-compd., left for 3 months at room temp.;
参考文献
Razuvaev, G. A.; Mar'in, V. P.; Vyshinskaya, L. I.; Grinval'd, I. I.; Spiridonova, N. N.
Journal of General Chemistry USSR (English Translation), 1987 , vol. 57, p. 1583 - 1591
Zhurnal Obshchei Khimii, 1987 , vol. 57, p. 1773 - 1782
