反应条件
in not given byproducts: (C2H5)2NH, H2O; under argon; 9.5 g hydroxymethylferrocene and 11.6 g 1,1'-bis(dimethyl(diethylamino)silyl)ferrocene are heated to 90-100°C; reaction mixt. distd. under vac.; in the distillate, vinylferrocene and 1,3-tetramethyldisiloxane ferrocenophane are found by chromy.; the latter is recrystd. from isopropyl alcohol; products identified by chromy., IR, and mass spectrometry;
参考文献
Buziashvili, V. I.; Kabanov, B. K.; Khananashvili, L. M.; Molchanov, B. V.; Tsomaya, M. I.
Journal of General Chemistry USSR (English Translation), 1988 , vol. 58, p. 87 - 90
Zhurnal Obshchei Khimii, 1988 , vol. 58, p. 100 - 104
