反应条件
water in tetrahydrofuran byproducts: poly(diphenylsiloxane); (N2); addn. of N2 sat. H2O to soln. of Cr-compd. in warm THF; filtration (Al2O3), removal of solvent (reduced pressure), recrystn. (ligroin); detn. by (1)H- and (13)C-NMR spectroscopy;
参考文献
Elschenbroich, Christoph; Hurley, James; Metz, Bernhard; Massa, Werner; Baum, Gerhard
Organometallics, 1990 , vol. 9, p. 889 - 897
