Fischer, E. O.; Muller, J.; Kuzel, P.
Revue de Chimie, Academie de la Republique Populaire Roumaine, 1962 , vol. 7, p. 827 - 834
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Gmelin Handbook: Cr: Org.Verb., 1.1.1.1.3, page 10 - 13
in gaseous matrix metal vaporizing (Nd(3+):YAG laser, 532 nm), C6H6 addn. (He carrier gas,room temp., partial pressure 70 Torr); not isolated, detd. by MS spectroscopy;
in toluene (N2); cocondensation of Cr, bimesityl and benzene during 1 h from a conic W-wire spiral and separation of heatable bimesityl and benzene vapour source in a static, evacuated reactor (cooled by N2(l)); warming to room temp.; addn. of solvent; filtration (silica gel); evapn. of solvent; sublimation of bimesityl, and compound 6 at 80°C; sublimation of compound 5 between 90-110°C; sublimation of complex 2 at 180°C;
参考文献
Journal of Organometallic Chemistry, , vol. 391, # 2 p. 195 - 208
in gas reactor was charged with vapours (Cr vapour from electrically heated W-wire basket/protective gas: Ar); reactor was allowed to thaw;; evapn. of excess arene; not isolated; identified by TLC and comparison;;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, p. 2391 - 2395
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2576 - 2579
