N,N-二甲基二茂铁甲胺合成路线 （共 30 条）
参考文献
Journal of Organometallic Chemistry, , vol. 37, p. 167 - 171
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 1631 - 1635
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 1776 - 1782
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 950 - 953
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 1045 - 1049
反应条件
in water addn. of concd. hydrochloric acid to ferrocene deriv., reflux for 1 h, cooling, satn. with H2S; filtering-off ppt. (H2S), washing in succession with water, acetone, and ethanol, neutralization of filtrate with 10percent aq. NaOH, extn. with Et2O, drying exts. over Na2SO4, evapn. to isolate ferrocene deriv.;
参考文献
Russian Journal of General Chemistry, , vol. 70, # 2 p. 291 - 297
反应条件
in water addn. of concd. hydrochloric acid to ferrocene deriv., reflux for 1 h, cooling, satn. with H2S; filtering-off ppt. (H2S), washing in succession with water, acetone, and ethanol, neutralization of filtrate with 10percent aq. NaOH, extn. with Et2O, drying exts. over Na2SO4, evapn. to isolate ferrocene deriv.;
参考文献
Russian Journal of General Chemistry, , vol. 70, # 2 p. 291 - 297
反应条件
in water addn. of concd. hydrochloric acid to ferrocene deriv., reflux for 1 h, cooling, satn. with H2S; filtering-off ppt. (H2S), washing in succession with water, acetone, and ethanol, neutralization of filtrate with 10percent aq. NaOH, extn. with Et2O, drying exts. over Na2SO4, evapn. to isolate ferrocene deriv.;
参考文献
Russian Journal of General Chemistry, , vol. 70, # 2 p. 291 - 297
反应条件
manganese(IV) oxide in chloroform activated MnO2, in boiling CHCl3;
参考文献
Gmelin Handbook: Fe: Org.Verb.A4, 5.1.4.1.3.2.3, page 45 - 48
反应条件
manganese(IV) oxide in chloroform activated MnO2, in boiling CHCl3, short react. time;
参考文献
Tetrahedron Letters, , p. 5885 - 5888
反应条件
manganese(IV) oxide in 1,2-dichloro-ethane with excess of activated MnO2, in boiling C2H4Cl2;
参考文献
Tetrahedron Letters, , p. 5885 - 5888
反应条件
potassium tert-butylate; oxygen in N,N,N',N',N'',N''-hexamethylphosphoric triamide 80°C;
参考文献
Gmelin Handbook: Fe: Org.Verb.A4, 5.1.4.1.3.2.3, page 45 - 48
反应条件
in water; acetonitrile
Kinetics; other Radiation; laser flash photolysis (0.6 μs laser pulse at ca. 200 mJ) react. of Cr complex with ferrocene deriv. in deaerated acetonitrile-H2O (70percent-30percent) at 25.+-.1°C; monitored by UV;
参考文献
Lee, Shoayung; Bakac, Andreja; Espenson, James H.
Inorganic Chemistry, 1989 , vol. 28, p. 1367 - 1369
