反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1: 50.5 percent / pentane / 100 h / Irradiation<br />2: 1.) MeLi / 1.) THF, 20 deg C, 2 h, 2.) 20 deg C, 15 h<br />3: 96.3 percent / SO<sub>2</sub> / 2 h / Ambient temperature<br />4: 1.) n-BuLi / 1.) THF, hexane, RT, 20 min, 2.) -78 deg C, 1 h<br /> <br />
参考文献
Salomon; Sachinvala; Roy; Basu; Raychaudhuri; Miller; Sharma Journal of the American Chemical Society, 1991 , vol. 113, # 8 p. 3085 - 3095
