(+)-3,3-二氯-2,N-环氧-外型-10,2-莰烷磺内酰胺合成路线 (共 2 条)
反应条件
potassium carbonate; 3-chloro-benzenecarboperoxoic acid in dichloromethane 18 h;
参考文献
Davis, Franklin A.; Weismiller, Michael C.
Journal of Organic Chemistry, 1990 , vol. 55, # 12 p. 3715 - 3717
反应条件
1: 1) 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU), 2) 1,3-dichloro-5,5-dimethylhydantoin (DCDMH) / 1) ethyl acetate, room temp., 30 min, 2) 20 - 25 deg C (ice-water bath), 90 min View Scheme
参考文献
Tetrahedron Letters, , vol. 33, # 2 p. 161 - 164