反应条件
n-BuLi; tosyl(toluene-p-sulphonyl)chloride in diethyl ether; hexane
N2, stirring of ferrocene and BuLi for 6 h, cooling to -78°C, addn. of chloride-component, stirring for 3 h, standing overnight; addn. oh water, filtn. (Celite), rapid chromy. (alumina (II), light petroleum), evapn., recrystn., separation of ferrocene (30percent) by chromy. (silica gel, hexane);
参考文献
Phillips, Leonidas; Lacey, Anthony R.; Cooper, Mervyn K.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 1383 - 1392