反应条件
Stage #1: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '8435405', constants.ctx, '0')">C{N(2,6-iPr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>)CH}2</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=0 - 20°C; Reformatsky Reaction; 24 h; Inert atmosphereGreen chemistry; <br />Stage #2: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1098214', constants.ctx, '0')">hydrogenchloride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>; <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />Reformatsky Reaction; 0.5 h; Inert atmosphereGreen chemistry; <br /> <br />
参考文献
Zou, Xiao-Lei; Du, Guang-Fen; Sun, Wan-Fu; He, Lin; Ma, Xiao-Wei; Gu, Cheng-Zhi; Dai, Bin Tetrahedron, 2013 , vol. 69, # 2 p. 607 - 612