4-(2-吡啶基)-苯甲醛合成路线 （共 28 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate in acetonitrile Suzuki coupling; 5 h; Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 3 p. 631 - 634
反应条件
1.1: toluene-4-sulfonic acid / water; methanol / 3 h / 20 °C 2.1: magnesium; iodine / tetrahydrofuran / 2 h / 20 °C / |Heating 2.2: 2.25 h / 20 °C 3.1: hydrogenchloride / water; tetrahydrofuran / |Cooling with ice View Scheme
参考文献
Organic Process Research and Development, , vol. 12, # 1 p. 69 - 75
反应条件
hydrogenchloride in tetrahydrofuran; water Cooling with ice;
参考文献
Fan, Xing; Song, Yan-Li; Long, Ya-Qiu
Organic Process Research and Development, 2008 , vol. 12, # 1 p. 69 - 75
反应条件
1.1: magnesium; iodine / tetrahydrofuran / 2 h / 20 °C / |Heating 1.2: 2.25 h / 20 °C 2.1: hydrogenchloride / water; tetrahydrofuran / |Cooling with ice View Scheme
参考文献
Organic Process Research and Development, , vol. 12, # 1 p. 69 - 75
反应条件
1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 36 h / 80 °C 2: water; calcium carbonate / 15 h / 100 °C View Scheme
参考文献
Dalton Transactions, , vol. 41, # 9 p. 2582 - 2591
反应条件
1: p-tolyl lithium; toluene 2: chromium (VI)-oxide; sulfuric acid; acetic acid View Scheme
参考文献
Journal of the Chemical Society, , p. 100,101
反应条件
chromium(VI) oxide; sulfuric acid; acetic acid Reagens 4:Acetanhydrid;
参考文献
Journal of the Chemical Society, , p. 100,101
反应条件
chromium(VI) oxide; sulfuric acid; acetic acid
参考文献
Journal of the Chemical Society, , p. 100,101
反应条件
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene in water; tert-butyl alcohol T=20°C; 2 h;
参考文献
Concert Pharmaceuticals Inc.
Patent: EP2003120 A1, 2008 ;
Location in patent: Page/Page column 20; 35; 37 ;
EP 2003120 A1
反应条件
sodium tetrahydroborate in ethanol T=20°C; 0.5 h;
参考文献
Zeng, Xianshun; Batsanov, Andrei S.; Bryce, Martin R.
Journal of Organic Chemistry, 2006 , vol. 71, # 26 p. 9589 - 9594
