反应条件
1: 3,5-dichlorophenylzinc bromide With CCl2CuLi2N in tetrahydrofuran T=-20 - 0°C; Negishi coupling reaction; Inert atmosphere; 2: benzoyl chloride in tetrahydrofuran T=-20 - 20°C; Negishi coupling reaction; 2 h; Inert atmosphere;
参考文献
Jin, Meng-Yi; Yoshikai, Naohiko
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 1972 - 1978