反应条件
1: nitric acid; tin(IV) chloride / dichloromethane / 20 °C / Cooling with ethylene glycol-dry ice
2: sodium dithionite / methanol; water / 2 h / 55 - 65 °C
3: formamide / 16 h / 150 °C
4: tetrachloromethane; triphenylphosphine / 1,2-dichloro-ethane / 80 °C
View Scheme
参考文献
Pham, Helen Trinh; Hanson, Robert N.; Olmsted, Sandra L.; Kozhushnyan, Anton; Visentin, Adam; Weglinsky, Paul J.; Massero, Chris; Bailey, Kristen
Tetrahedron Letters, 2011 , vol. 52, # 10 p. 1053 - 1056
