2,5-脱水-d-甘露糖肟合成路线 （共 4 条）
反应条件
hydroxylamine hydrochloride; sodium acetate in ethanol Condensation; 1.5 h;
参考文献
Abdel-Rahman, Adel A.-H.; El Ashry, El Sayed H.; Schmidt, Richard R.
Carbohydrate Research, 1999 , vol. 315, # 1-2 p. 106 - 116
反应条件
1.1: sodium nitrite / H2O / 4 h / 0 °C 1.2: 87 percent / Dowex 1x8-50, CO3(2-) 2.1: 87 percent / hydroxylamine hydrochloride; sodium acetate / methanol / 6 h / 20 °C View Scheme
参考文献
Plutschack, Matthew B.; McQuade, D. Tyler; Valenti, Giulio; Seeberger, Peter H.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 2022 - 2027
反应条件
1: NaNO2, AcOH / H2O 2: NH2OH*HCl, NaOMe / methanol / 25 °C View Scheme
参考文献
Jung, Michael E.; Trifunovich, Ivan D.; Gardiner, John M.; Clevenger, Gary L.
Journal of the Chemical Society, Chemical Communications, 1990 , # 1 p. 84 - 85
反应条件
formic acid; hydrogen; palladium on activated charcoal in methanol T=20°C; Hydrogenolysis; P=760 Torr; 10 h;
参考文献
Claustre, Samantha; Bringaud, Frederic; Azema, Laurent; Baron, Rudi; Perie, Jacques; Willson, Michele
Carbohydrate Research, 1999 , vol. 315, # 3-4 p. 339 - 344
