(S)-1-[2-(三氟甲基)苯基]乙胺合成路线 （共 7 条）
反应条件
5 Pd(II)/C(eggshell); hydrogen in methanol T=60°C; P=11251.1 Torr; 24 h; optical yield given as percent ee;
参考文献
Nugent, Thomas C.; Negru, Daniela E.; El-Shazly, Mohamed; Hu, Dan; Sadiq, Abdul; Bibi, Ahtaram; Umar, M. Naveed
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2085 - 2092
反应条件
1: 76 percent / zinc chloride / toluene / 44 h / Heating 2: sodium borohydride / methanol / 0 °C 3: hydrogen; acetic acid; water / 5 percent Pd/C NX-type / methanol / 12 h / 60 °C / 3750.3 Torr View Scheme
参考文献
Organic Letters, , vol. 5, # 7 p. 1007 - 1010
反应条件
1: sodium borohydride / methanol / 0 °C 2: hydrogen; acetic acid; water / 5 percent Pd/C NX-type / methanol / 12 h / 60 °C / 3750.3 Torr View Scheme
参考文献
Organic Letters, , vol. 5, # 7 p. 1007 - 1010
反应条件
borane; (S)-(-)-2-amino-3-methyl-1,1-diphenylbutan-1-ol in tetrahydrofuran Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 112, # 15 p. 5741 - 5747
反应条件
1: sodium hydroxide / water; ethyl acetate 2: 5 Pd(II)/C(eggshell); hydrogen / methanol / 24 h / 60 °C / 11251.1 Torr View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 11-12 p. 2085 - 2092
反应条件
sodium hydroxide in dichloromethane; water
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 11-12 p. 2085 - 2092
反应条件
hydrogenchloride in dichloromethane; water
参考文献
Nugent, Thomas C.; Marinova, Sofiya M.
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-Z0768-FA, p. 153 - 166
