tetrabutyl-ammonium chloride in water Electrolysis; a soln. of the acid was electrolyzed at Cu anode for 6 h (70 V); concn. of soln. from anode compartment, cooling, filtn., washing with water, elem. anal.;
参考文献
Zelenov; Shabanova; Tsokur
Russian Journal of General Chemistry, 2008 , vol. 78, # 11 p. 2166 - 2166
benzoic acid in acetone Electrolysis; 5 h, initial voltage 10 V; mixture was filtered, solvent evapd. in vacuo, salt dissolved in diethylether,recrystn. from ethanol; elem.anal.;
参考文献
Kumar, N.; Tuck, Dennis G.; Watson, Katherine D.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 740 - 743
in methanol Electrochem. Process; Cu anode; working soln.: C11H15NO in MeOH, Et4NClO4 as a conducting additive, at current strength of 40 mA, voltage of 15 V for 1 h at room temp.; ppt. filtered off; recrystd. from EtOH, dried in vac. desiccator; elem. anal.;
dioxygen in pyridine stirred at room temp. under an atmosphere of oxygen for 3.5 h; evapn. of pyridine under reduced pressure, triturated with diethyl ether, filtered off, washed with diethyl ether, dried in vac.; elem. anal.;
参考文献
Speier, Gabor; Tyeklar, Zoltan
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 2663 - 2668
