in further solvent(s) stirring of a mixt. of Cu, urea and C8H3ClO3 in trichlorobenzene at ambient temp. for 30 minutes; heating at 175-180°C for 4 h; evapn.; heating with 5percent HCl; heating with 2percent aq. Na2CO3;; washing with H2O and ethanol; drying at 95-100°C;;
参考文献
Shigemitsu, M.
Bulletin of the Chemical Society of Japan, 1959 , vol. 32, p. 691 - 693
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Gmelin Handbook: Cu: MVol.B4, 145, page 1768 - 1770
in neat (no solvent) simultanous thermal vaporisation (1E-4 mmHg); vibrational spectroscopy;
参考文献
Kuzharov, A. S.; Kut'kov, A. A.; Suchkov, V. V.
Russian Journal of Physical Chemistry, 1980 , vol. 54, # 12 p. 1784 - 1786
Zhurnal Fizicheskoi Khimii, 1980 , vol. 54, p. 3118 - 3122
