[2-(2-氨基乙氧基)乙基]氨基甲酸叔丁酯合成路线 （共 8 条）
反应条件
1: With triphenylphosphine in tetrahydrofuran T=20°C; 2 h; 2: With water in tetrahydrofuran T=20°C;
参考文献
EP1745802 A1, ;
Page/Page column 17 ;
反应条件
sodium hydroxide in tetrahydrofuran; methanol T=20°C;
参考文献
Journal of Organic Chemistry, , vol. 72, # 7 p. 2289 - 2296
反应条件
sodium hydroxide in tetrahydrofuran; methanol T=20°C;
参考文献
Tetrahedron Letters, , vol. 47, # 17 p. 2915 - 2919
反应条件
methylamine in water T=20°C;
参考文献
EP2123283 A1, ;
Page/Page column 15 ;
反应条件
sodium hydroxide in tetrahydrofuran; methanol T=20°C; 24 h;
参考文献
European Journal of Organic Chemistry, , # 17 p. 3004 - 3014
反应条件
1: sodium hydroxide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere 3: sodium azide / N,N-dimethyl-formamide / 1.5 h / 90 °C 4: hydrogen / palladium 10 on activated carbon / methanol / 18.5 h / 1500.15 Torr View Scheme
反应条件
1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere 2: sodium azide / N,N-dimethyl-formamide / 1.5 h / 90 °C 3: hydrogen / palladium 10 on activated carbon / methanol / 18.5 h / 1500.15 Torr View Scheme
反应条件
1: sodium azide / N,N-dimethyl-formamide / 1.5 h / 90 °C 2: hydrogen / palladium 10 on activated carbon / methanol / 18.5 h / 1500.15 Torr View Scheme
